Pesticide Synthesis Handbook by Thomas A. Unger

By Thomas A. Unger

The target of this instruction manual is to explain the elemental synthesis route(s) for the manufacture of 687 insecticides. vital additional info comprises the 5 appendices:
I. typical Names: The regular identify Appendix shows the chemical functionality of the compound. If the compound has a couple of functionality, all services are indicated. thus, the synthesis direction of the compound is located less than the 1st functionality indicated during this Appendix.
II. exchange Names: whilst basically the alternate identify of the product is understood, the corresponding prevalent identify is located during this Appendix.
III. uncooked fabrics and Intermediates: This Appendix lists all insecticides, the synthesis of which makes use of a given uncooked fabric or intermediate.
IV. Synthesis of uncooked fabrics and Inter-mediates: The synthesis routes of uncooked fabrics and Intermediates are offered during this Appendix.
V. Chemical services: This Appendix lists all items that have an analogous chemical functionality. The systhesis route(s) for every product are defined less than the heading of the most functionality. whilst a product has extra then one major chemical functionality, it's indexed less than all its functions.

An abbreviated Contents is indexed less than; the quantity in ( ) point out the variety of insecticides in that type, whose synthesis is defined.

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6 dimethyl aniline - I mC I C-I methoxy acetaldehyde 1t2 0 cl- "~/c-~ ' C"- ' C~ 0--- I --. -@, 0=- l C . -I N-- C--- "" I , // I \ Cl-- c-- c dimethachlor O C-I Cl chloro acetyl chloride Pretilachlor Uses: herbicide, Trade names : Type: rice Rifit (Ciba) ami d e Synthesis : As d i m e t h a c h l o r I I I I i/,o -- c-- c-- c-- o-- c-- c I I l I \ with propoxy acetaldehyde I Cl--c--c I N and -c-c-~c-c_ I I I . 6 diethyl anil ine I , ~ - - N"1 , , , i i I c - - c - - o - - i ~ " c--c-- , > pretilachlor ' ' I i 21 22 Pesticides Synthesis Handbook alternate route : \/ I N I I ~ I I i C--C--O--C--C-- I --C-- N I ' f I o =ffiS ~ - o I 0 I -C-I --C-.

6 diethyl anil ine I , ~ - - N"1 , , , i i I c - - c - - o - - i ~ " c--c-- , > pretilachlor ' ' I i 21 22 Pesticides Synthesis Handbook alternate route : \/ I N I I ~ I I i C--C--O--C--C-- I --C-- N I ' f I o =ffiS ~ - o I 0 I -C-I --C-. I 0 i # Cl--c--c I \ I I - - C =- --C"- I O Cl i I p. toluene sulfonic acid 2 propoxy ethyl ester pretilachlor Propisochlor Uses: herbicide, maize, sunflowers, soyabeans, potatoes Trade names: Type: Proponit (Nitrokemia) amide Synthesis: I --C-- As dimethaehlor with ---C----C----O----C I I O \ isopropyoxy formaldehyde \/ N and --c--c--f/"x ) - - c - 2 methyl 6 ethyl aniline O II CI-- cI --c l j \ ll~ N C I --C-- i I o--c--et I -, propisochlor I I C-- Amides and Similar Functions Diphenamid Uses: herbicide, cotton, soyabeans, potatoes, fruit, ornamentals, vegetables, tobacco Dymid (Lilly), Enide (Up John) names : Trade Type: amide Synthesis : XC~.

I Cl \ N ~' C - - Cram C - - ' ' ~ - cffi c I d ia I ly I amine dichlormid I I 17 18 Pesticides Synthesis Handbook Diethatyl-Ethyl Uses: herbicide, Trade names : Type: potatoes, Antor red beet, soyabeans, sugarbeet, wheat (NorAm) amide Synthesis: o ! \ , C--C-- t I o + el- ! 6 dimethyl aniline - I mC I C-I methoxy acetaldehyde 1t2 0 cl- "~/c-~ ' C"- ' C~ 0--- I --. -@, 0=- l C . -I N-- C--- "" I , // I \ Cl-- c-- c dimethachlor O C-I Cl chloro acetyl chloride Pretilachlor Uses: herbicide, Trade names : Type: rice Rifit (Ciba) ami d e Synthesis : As d i m e t h a c h l o r I I I I i/,o -- c-- c-- c-- o-- c-- c I I l I \ with propoxy acetaldehyde I Cl--c--c I N and -c-c-~c-c_ I I I .

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